Hydrochloric Acid → HCID 6102335, compound

HRID 1987678Notes

Reaction equation

HRID 1987678 reaction equation
CC1(C)[O:7][C@@H:6]2[C@H:8]([OH:13])[C@H:9]([OH:12])[CH2:10][O:11][C@H:5]2[CH2:4][O:3]1.Cl>CO>[OH:3][CH2:4][C@H:5]1[C@H:6]([OH:7])[C@H:8]([OH:13])[C@H:9]([OH:12])[CH2:10][O:11]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 57723934HCID 57723934, compound

Product 1

HCID 6102335HCID 6102335, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of (+)-(4aS,7R,8R,8aR)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (28 mg, 0.14 mmol) in MeOH (2 mL) was added a solution of methanolic HCl (0.4 mL, prepared from 0.5 mL conc. HCl in 30 mL of MeOH). The solution was stirred for 1H at ambient temperature and concentrated in vacuo.

Workup

  1. concentrationconcentrated in vacuo

Sources & evidence

ORD record
ord-5d2bb3f71b9e4ba182fb2aafe95e0912
Source dataset
uspto-grants-2009_06
Patent number
US07550607B2

Reaction notes

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