HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11829766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57723960 | HCID 57723960 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 11829766 | HCID 11829766 | — |
Reaction Steps
To a solution of (+)-(4aS,7R,8R,8aS)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (36 mg, 0.18 mmol) in MeOH (2 mL) was added a solution of methanolic HCl (0.5 mL, prepared from 0.5 mL conc. HCl in 30 mL of MeOH). The solution was stirred for 1 H at ambient temperature and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550607B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-d695b42241c34609aa09aca2d32e2d48 |
| Source note | uspto-grants-2009_06 |