Hydrochloric Acid → HCID 11829766, compound

HRID 1987680Notes

Reaction equation

HRID 1987680 reaction equation
CC1(C)[O:7][C@H:6]2[C@H:8]([OH:13])[C@H:9]([OH:12])[CH2:10][O:11][C@H:5]2[CH2:4][O:3]1.Cl>CO>[OH:3][CH2:4][C@H:5]1[C@@H:6]([OH:7])[C@H:8]([OH:13])[C@H:9]([OH:12])[CH2:10][O:11]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 57723960HCID 57723960, compound

Product 1

HCID 11829766HCID 11829766, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

To a solution of (+)-(4aS,7R,8R,8aS)-2,2-dimethyl-hexahydro-pyrano[3,2-d][1,3]dioxine-7,8-diol (36 mg, 0.18 mmol) in MeOH (2 mL) was added a solution of methanolic HCl (0.5 mL, prepared from 0.5 mL conc. HCl in 30 mL of MeOH). The solution was stirred for 1 H at ambient temperature and concentrated in vacuo.

Workup

  1. concentrationconcentrated in vacuo

Sources & evidence

ORD record
ord-d695b42241c34609aa09aca2d32e2d48
Source dataset
uspto-grants-2009_06
Patent number
US07550607B2

Reaction notes

Loading…