HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 29972132, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57723947 | HCID 57723947 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 29972132 | HCID 29972132 | — |
Reaction Steps
To a solution of (−)-(4aR,7S,8S,8aS)-2,2-dimethyl-hexahydropyrano[3,2-d][1,3]dioxine-7,8-diol (20 mg, 0.09 mmol) in MeOH (2 mL) was added a solution of methanolic HCl (0.5 mL, prepared from 0.5 mL conc. HCl in 30 mL of MeOH). The solution was stirred for 1H at ambient temperature and concentrated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07550607B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-f7c24f51373c4229ba76035dcc6cebe1 |
| Source note | uspto-grants-2009_06 |