6-Bromo-2-naphthoyl chloride → 6-Bromo-naphthalene-2-carboxylic acid (2-acetylamino-benzothiazol-4-yl)-amide

Participants

Reaction Steps

This material was prepared analogous to the procedure described for Example 1(b). 6-Bromo-naphthalene-2-carbonyl chloride, Example 1(a), (98 mg, 0.36 mmol) reacted with N-(4-amino-benzothiazol-2-yl)-acetamide (50 mg, 0.24 mmol, prepared according to the procedure described in WO03099284) to give the title compound as a solid. Mp 241.6° C. MS (ESI, pos. ion.) m/z: 441 (M+1).

Provenance & Evidence