HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69066270, compound → HCID 43186111, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69066270 | HCID 69066270 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 43186111 | HCID 43186111 | 99% |
Reaction Steps
To a solution of 3-(4-nitrophenoxy)-dihydrofuran-2-one (47 mg, 0.21 mmol) in EtOH (3 mL) was added palladium hydroxide (<1 mg). The reaction flask was evacuated and purged with H2 and then stirred at room temperature under a H2 atmosphere for 1 hour. The catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to provide the desired product (40 mg, 99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07553842B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-cf7353b6bc414de9acbd82066b310e9a |
| Source note | uspto-grants-2009_06 |