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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1987824Generated: November 3, 2026

HCID 69066270, compound → HCID 43186111, compound

https://huagongshe.com/reaction/1987824

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69066270HCID 69066270—
CatalystPalladium hydroxideHCID 9942167—
SolventEthanolHCID 702—
ProductHCID 43186111HCID 4318611199%

Reaction Steps

To a solution of 3-(4-nitrophenoxy)-dihydrofuran-2-one (47 mg, 0.21 mmol) in EtOH (3 mL) was added palladium hydroxide (<1 mg). The reaction flask was evacuated and purged with H2 and then stirred at room temperature under a H2 atmosphere for 1 hour. The catalyst was removed by filtration and the filtrate was concentrated under reduced pressure to provide the desired product (40 mg, 99%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07553842B2
Source datasetuspto-grants-2009_06
ORD IDord-cf7353b6bc414de9acbd82066b310e9a
Source noteuspto-grants-2009_06