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HRID1987835

反应详情

EQUATION

反应方程式

HRID 1987835 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)CCl
HCID6571

1-Chloropropan-2-one

C3H5ClO

结构：Cc1ccc(NC(=O)OC(C)(C)C)cn1
HCID23090429

tert-Butyl (6-methylpyridin-3-yl)carbamate

C11H16N2O2

PRODUCTS

生成物

1
结构：Cc1cc2ccc(NC(=O)OC(C)(C)C)cn2c1
HCID57725262

未命名化合物

收率 31%

PROCEDURE

实验过程

This compound is obtained according to the same procedure as the compound of Preparation III using the Tschitschibabin reaction, starting with 5.79 g of tert-butyl (6-methylpyridin-3-yl)carbamate [described in J. Med. Chem.; (2000), 43, 5017-5029] and chloroacetone. 1.96 g of a pasty residue are obtained.

WORKUP

后处理

  1. customThis compound is obtained
  2. customthe Tschitschibabin reaction