HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloroacetone → HCID 57725262, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloroacetone | HCID 6571 | — |
| Reactant | tert-Butyl (6-methylpyridin-3-yl)carbamate | HCID 23090429 | — |
| Product | HCID 57725262 | HCID 57725262 | 31% |
Reaction Steps
This compound is obtained according to the same procedure as the compound of Preparation III using the Tschitschibabin reaction, starting with 5.79 g of tert-butyl (6-methylpyridin-3-yl)carbamate [described in J. Med. Chem.; (2000), 43, 5017-5029] and chloroacetone. 1.96 g of a pasty residue are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07553845B2 |
| Source dataset | uspto-grants-2009_06 |
| ORD ID | ord-e9269e60a04c460f905155d344f4031b |
| Source note | uspto-grants-2009_06 |