Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 11523830 | HCID 11523830 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86607551 | HCID 86607551 | — |
Reaction Steps
0.19 mL (2.02 mmol) of dimethyl sulfate is added to a mixture of 705 mg (1.84 mmol) of methyl [8-hydroxy-3-(3-methoxy-4-nitrobenzoyl)-2-methylindolizin-1-yl]carboxylate obtained in Example 2, in 10 mL of acetone with 330 mg (2.39 mmol) of potassium carbonate and the medium is heated at 60° C. for 6 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07553845B2 |
|---|
| Source dataset | uspto-grants-2009_06 |
|---|
| ORD ID | ord-ac74a1b3d2964e838004891524c75be3 |
|---|
| Source note | uspto-grants-2009_06 |
|---|
