Hydrochloric Acid → HCID 178492044, compound

HRID 1987956Notes

Reaction equation

HRID 1987956 reaction equation
[CH2:1]([NH:8][C:9]1[CH:13]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:12]([C:20]2[CH:25]=[CH:24][C:23]([O:26][CH3:27])=[CH:22][CH:21]=2)[C:11](=[O:28])[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[ClH:29]>CO>[ClH:29].[CH2:1]([NH:8][C:9]1[CH:13]([C:14]2[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=2)[N:12]([C:20]2[CH:25]=[CH:24][C:23]([O:26][CH3:27])=[CH:22][CH:21]=2)[C:11](=[O:28])[N:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 178492043HCID 178492043, compound

Product 1

HCID 178492044HCID 178492044, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

20 mg of (Rac)-4-benzylamino-1-(4-methoxy-phenyl)-5-phenyl-1,5-dihydro-imidazol-2-one was stirred for 2 hours at room temperature in a solution of 3N HCl in methanol. Evaporation of the solvent gave the title compound. m/z (EI) 372.2 (100%, M+H+).

Workup

  1. customEvaporation of the solvent

Sources & evidence

ORD record
ord-c7948d82489a44929bff53e8ecad8fb6
Source dataset
uspto-grants-2009_06
Patent number
US07553862B2

Reaction notes

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