Ammonia → HCID 178461419, compound

Participants

Reaction Steps

The title compound was prepared using the procedure described in Example 1C except substituting the product from Example 13A for the product from Example 1B. 1H NMR (300 MHz, CD3OD) δ 1.36 (d, J=6 Hz, 3 H), 1.72 (m, 1 H), 2.01 (m, 2 H), 2.24 (m, 1 H), 2.55 (m, 1 H), 2.63 (m, 1 H), 2.78 (m, 2 H), 3.02 (m, 1 H), 3.25 (m, 1 H), 3.42 (m, 1 H), 3.69 (m, 1 H), 3.90 (m, 1 H), 7.47 (d, J=9 Hz, 2 H), 7.68 (d, J=9 Hz, 2 H), 7.80 (AB q, 4 H); (DCl/NH3) m/z 317 (M+H)+.

Provenance & Evidence