Ammonia → HCID 178461417, compound

Participants

Reaction Steps

The title compound was prepared using the procedure described in Example 1B except substituting the product from Example 22C for the product from Example 1A. 1H NMR (300 MHz, CD3OD) δ 1.12 (d, J=6 Hz, 3 H), 1.48 (m, 1 H), 1.78 (m, 2 H), 2.00 (m, 1 H), 2.23 (m, 1 H), 2.36 (m, 2 H), 2.59 (m, 3 H), 3 H), 3.03 (m, 1 H), 3.34 (m, 1 H), 3.48 (m, 1 H), 7.06 (dd, J=9 Hz, J=3 Hz, 1 H), 7.17 (dd, J=9 Hz, J=3 Hz, 1 H), 7.53 (t, J=9 Hz, 1 H); (DCl/NH3) m/z 312 (M+H)+.

Provenance & Evidence