HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonyl alcohol → 4-[(2H-1,3-Benzodioxol-5-yl)methoxy]-3-nitropyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonyl alcohol | HCID 10322 | — |
| Reactant | 4-Chloro-3-nitropyridine | HCID 2735781 | — |
| Product | 4-[(2H-1,3-Benzodioxol-5-yl)methoxy]-3-nitropyridine | HCID 68702496 | — |
Reaction Steps
In accordance with the same procedures as in Preparation 2, except for using 4-chloro-3-nitropyridine (3.0 g, 18.92 mmol) prepared in Step 1 of Preparation 1 and piperonyl alcohol (3.45 ml, 18.92 mmol), the titled compound was obtained as a yellow solid. (3.08 g, 88.6%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642269B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-fe6f388fe6c44081b5017dae111c3eac |
| Source note | uspto-grants-2010_01 |