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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1988841Generated: November 4, 2026

Methanesulfonic Acid → HCID 86615031, compound

https://huagongshe.com/reaction/1988841

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanesulfonic AcidHCID 6395—
ReactantHCID 11653485HCID 11653485—
SolventEthyl AcetateHCID 8857—
ProductHCID 86615031HCID 8661503185.1%

Reaction Steps

0.039 ml of Methanesulfonic acid was added at room temperature to a solution of 7-(4-fluorobenzyloxy)-1-(2-methoxyethyl)-2,3-dimethyl-1H-pyrrolo[3,2-b]pyridine (200 mg, 0.609 mmol) prepared in Example 122 in 10 ml of ethyl acetate and then stirred for 24 hours at the same temperature. The resulting solid was filtered to give the titled compound as a white solid. (Yield: 85.1%)

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07642269B2
Source datasetuspto-grants-2010_01
ORD IDord-d034238beb534662ac33570368d238ab
Source noteuspto-grants-2010_01