HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonic Acid → HCID 86615031, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonic Acid | HCID 6395 | — |
| Reactant | HCID 11653485 | HCID 11653485 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 86615031 | HCID 86615031 | 85.1% |
Reaction Steps
0.039 ml of Methanesulfonic acid was added at room temperature to a solution of 7-(4-fluorobenzyloxy)-1-(2-methoxyethyl)-2,3-dimethyl-1H-pyrrolo[3,2-b]pyridine (200 mg, 0.609 mmol) prepared in Example 122 in 10 ml of ethyl acetate and then stirred for 24 hours at the same temperature. The resulting solid was filtered to give the titled compound as a white solid. (Yield: 85.1%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642269B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-d034238beb534662ac33570368d238ab |
| Source note | uspto-grants-2010_01 |