HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium methanethiolate → HCID 18434372, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium methanethiolate | HCID 4378561 | — |
| Reactant | 4-Bromo-1-(bromomethyl)-2-nitrobenzene | HCID 12761378 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 18434372 | HCID 18434372 | 105.8% |
Reaction Steps
A suspension of 4-bromo-1-(bromomethyl)-2-nitrobenzene (1.0 g) and sodium methanethiolate (0.285 g) in tetrahydrofuran (20 ml) was stirred under nitrogen for 60 h. The solvent was evaporated, chloroform (50 ml) was added and the rsidual solid was removed by filtration. The filtrate was comncentrated under vacuum to give the title compound (0.89 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642276B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-9f04f6de723e4ac1822b9b8dab7cc130 |
| Source note | uspto-grants-2010_01 |