Acetic Acid → HCID 68528074, compound

HRID 1989090Notes

Reaction equation

HRID 1989090 reaction equation
[C:1]([OH:4])(=[O:3])[CH3:2].[CH3:5][N:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1>O.C(#N)C>[C:1]([OH:4])(=[O:3])[CH3:2].[CH3:5][N:6]1[CH2:11][CH2:10][CH2:9][CH2:8][CH2:7]1

Participants

5

Reactant 2

HCID 176Acetic AcidHCID 12291N-Methylpiperidine

Product 1

HCID 68528074HCID 68528074, compound

Reagents, catalysts & solvents 2

HCID 962WaterSolvent2×HCID 6342AcetonitrileSolvent

Procedure

A stock solution of 1 molar methylpiperidine acetate was prepared by mixing one equivalent of glacial acetic acid in an appropriate volume of water and slowly adding one equivalent of 1-methylpiperidine. The pH of the solution is 7. The stock solution was diluted with an appropriate volume of water or acetonitrile to working concentration.

Workup

  1. concentrationconcentration

Sources & evidence

ORD record
ord-c6ab14c9b44b43829188b0ceeb8134c3
Source dataset
uspto-grants-2010_01
Patent number
US07642344B2

Reaction notes

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