HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyanophenylboronic acid → HCID 57469007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyanophenylboronic acid | HCID 2734325 | — |
| Reactant | Trifluoro-methanesulfonic acid 6-methyl-4-(4-trifluoromethyl-phenyl)-pyridin-2-yl ester | HCID 57468647 | — |
| Product | HCID 57469007 | HCID 57469007 | — |
Reaction Steps
The title compound was prepared trifluoro-methanesulfonic acid 6-methyl-4-(4-trifluoromethyl-phenyl)-pyridin-2-yl ester (example A.32) (5.00 g, 13 mmol) and commercially available 3-cyanophenylboronic acid (1.67 g, 14.3 mmol) according to the general procedure VI. Obtained as a white solid (3.00 g, 68%). MS (ISP) 339.1 [(M+H)+]; mp 140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642264B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-afe7cc935d624641aa8c87a2d6bfcfb5 |
| Source note | uspto-grants-2010_01 |