HCID 12518666, compound → HCID 86615571, compound

Participants

Reaction Conditions

Reaction Steps

Under an argon gas flow, 70 g (0.24 mol) of 2,8-dimethoxy-5,6,11,12-tetrahydrochrysene and 50 g of Pd/C were charged into a 5 L round bottom flask equipped with a condenser, and heated at 200° C. for 1 h. Thereafter, the obtained reaction mixture was heated to 300° C. and sublimated. The resultant reaction product was recrystallized with acetic acid, thereby obtaining 24 g of the aimed product (yield: 35%).

Provenance & Evidence