HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68524247, compound → HCID 68526305, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68524247 | HCID 68524247 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 68526305 | HCID 68526305 | — |
Reaction Steps
A glass reaction vessel was charged with 1 g of 4-isopropylidene-1-methyl-2-cyclohexenylmethanol, the catalyst shown in Table 1 and 20 mL of isopropanol, and the contents of the reaction vessel were reacted with each other at a pressure of from 0.2 to 0.3 MPa and a temperature of 25° C. for the time period shown in Table 1. Thereafter, the reaction mixture was filtered to remove the catalyst therefrom, and then concentrated to obtain 4-isopropyl-1-methyl-3-cyclohexenylmethanol. The amount of hydrogen consumed and the yield of the 4-isopropyl-1-methyl-3-cyclohexenylmethanol are shown in Table 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07642385B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-a3f5c210b89744e7b6822262f1afc9ca |
| Source note | uspto-grants-2010_01 |