HCID 68524247, compound → HCID 68526305, compound

A glass reaction vessel was charged with 1 g of 4-isopropylidene-1-methyl-2-cyclohexenylmethanol, the catalyst shown in Table 1 and 20 mL of isopropanol, and the contents of the reaction vessel were reacted with each other at a pressure of from 0.2 to 0.3 MPa and a temperature of 25° C. for the time period shown in Table 1. Thereafter, the reaction mixture was filtered to remove the catalyst therefrom, and then concentrated to obtain 4-isopropyl-1-methyl-3-cyclohexenylmethanol. The amount of hydrogen consumed and the yield of the 4-isopropyl-1-methyl-3-cyclohexenylmethanol are shown in Table 1.

1. customA glass reaction vessel
2. customthe contents of the reaction vessel were reacted with each other at a pressure of from 0.2 to 0.3 MPa
3. customa temperature of 25° C.
4. filtrationThereafter, the reaction mixture was filtered
5. customto remove the catalyst
6. concentrationconcentrated

ORD record

ord-a3f5c210b89744e7b6822262f1afc9ca

Source dataset

uspto-grants-2010_01

DOI

10.6084/m9.figshare.5104873.v1

Patent number

US07642385B2