HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 59128613, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86610100 | HCID 86610100 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 59128613 | HCID 59128613 | — |
Reaction Steps
4.6 ml (9.17 mmol) of a solution of methylamine (2M) in tetrahydrofuran are added to a solution of 1.0 g (3.06 mmol) of ethyl ({[2-(6-phenylpyrid-3-yl)ethyl]amino}carbonyl)-oxyacetate, obtained in stage 1.3., in 6 ml of methanol. Stirring is continued at ambient temperature for 4 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645757B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-36acfbdf53254cf4959291d22bcfcc0f |
| Source note | uspto-grants-2010_01 |