HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole → HCID 13340133, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole | HCID 798 | — |
| Reactant | 1,4-Dibromobutane | HCID 8056 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13340133 | HCID 13340133 | — |
Reaction Steps
0.96 g (17.07 mmol) of sodium hydroxide is added in small portions to a solution, cooled by a bath of ice-cold water, of 2 g (17.07 mmol) of 1H-indole and of 1.15 ml (51.22 mmol) of 1,4-dibromobutane in 80 ml of dimethylformamide. The bath is removed and stirring is continued at ambient temperature for 15 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645757B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-4685b173ec6b4b489e5eefb0aef44c32 |
| Source note | uspto-grants-2010_01 |