HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glyoxylic Acid → HCID 10822776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glyoxylic Acid | HCID 760 | — |
| Reactant | 1-(p-Methoxyphenyl)-2-propanone | HCID 31231 | — |
| Product | HCID 10822776 | HCID 10822776 | — |
Reaction Steps
16.42 g (0.10 mol) of 4-methoxyphenylacetone and an aqueous solution of 45% glyoxylic acid (19.4 ml, 0.11 mol) were stirred overnight at 100° C. The reaction liquid was concentrated under reduced pressure to obtain a crude product of 5-hydroxy-4-(4-methoxyphenyl)-5-methyl-5H-furan-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645756B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-bab1986a345a4bc3844caff7dc58b182 |
| Source note | uspto-grants-2010_01 |