Hydrogen Bromide → HCID 178419736, compound

Participants

Reaction Steps

47% hydrobromic acid was added to 141 mg of 6-(6-methoxypyridin-3-yl)-[1,2,4]triazolo[3,4-a]phthalazine, and refluxed for 4 hours. The reaction liquid was concentrated under reduced pressure, and ether was added to the resulting residue. The resulting solid was taken out through filtration to obtain 250 mg of 5-[1,2,4]triazolo[3,4-a]phthalazin-6-ylpyridin-2-ol hydrobromide as a brown solid.

Provenance & Evidence