HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylvanillin → HCID 86607629, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylvanillin | HCID 8467 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Bromocyclopropane | HCID 78037 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 86607629 | HCID 86607629 | — |
Reaction Steps
The title compound was prepared analogously to intermediate 2 (4-methoxy-3-propoxy-benzaldehyde) by reaction of 3-ethoxy-4-hydroxy-benzaldehyde with cyclopropyl bromide in DMF using K2CO3 as base. MS (ISP): 206.9 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645753B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-97ddb85d875840c092fd9fd412abfdcf |
| Source note | uspto-grants-2010_01 |