HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → 3-Ethoxy-4,5-dihydroxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,4,5-Trihydroxybenzaldehyde | HCID 83651 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | 3-Ethoxy-4,5-dihydroxybenzaldehyde | HCID 13017490 | — |
Reaction Steps
The title compound was prepared analogously to intermediate 2 (4-methoxy-3-propoxy-benzaldehyde) by reaction of 3,4,5-trihydroxybenzaldehyde with ethyl iodide in DMF using K2CO3 as base. MS (ISN): 181.1 [M−H]−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645753B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-1e6d564eb9da4ed9a64a578b8b18448d |
| Source note | uspto-grants-2010_01 |