Methyl iodide → HCID 11469564, compound

HRID 1990905Notes

Reaction equation

HRID 1990905 reaction equation
[C:1]([C:4]1[C:9]2[NH:10][C:11](=[O:13])[O:12][C:8]=2[CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].CI.[K].[CH3:17]C(C)([O-])C>CN(C)C=O>[C:1]([C:4]1[C:9]2[N:10]([CH3:17])[C:11](=[O:13])[O:12][C:8]=2[CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2]

Participants

5

Reactant 3

HCID 6328Methyl iodideHCID 99897794-Acetyl-1,3-benzoxazol-2(3H)-oneHCID 50987170Potassium tertbutoxide

Product 1

HCID 11469564HCID 11469564, compound

Reagents, catalysts & solvents 1

HCID 6228DimethylformamideSolvent

Procedure

Prepared by reacting 4-acetyl-3H-benzoxazol-2-one with methyl iodide in the presence of potassium-tert.-butoxide in N,N-dimethylformamide at ambient temperature.

Workup

  1. customPrepared
  2. customat ambient temperature

Sources & evidence

ORD record
ord-115e60ea7db347318a1505b15f298c7f
Source dataset
uspto-grants-2010_01
Patent number
US07645763B2

Reaction notes

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