HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59128690, compound → HCID 59128706, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59128690 | HCID 59128690 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 59128706 | HCID 59128706 | — |
Reaction Steps
A mixture of 96 (32 mg, 0.073 mmol) and Pd(OH)2 (1.0 mg, 7.3 μmol) in MeOH (2.0 mL) was stirred under H2 at r.t. for 30.5 h. The mixture was filtered through Celite and concentrated to afford 97, which was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645769B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-58326b8d41ae4f61a5d37376fe6aabfa |
| Source note | uspto-grants-2010_01 |