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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1991143Generated: November 1, 2026

HCID 59128690, compound → HCID 59128706, compound

https://huagongshe.com/reaction/1991143

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59128690HCID 59128690—
CatalystPalladium hydroxideHCID 9942167—
SolventMethanolHCID 887—
ProductHCID 59128706HCID 59128706—

Reaction Steps

A mixture of 96 (32 mg, 0.073 mmol) and Pd(OH)2 (1.0 mg, 7.3 μmol) in MeOH (2.0 mL) was stirred under H2 at r.t. for 30.5 h. The mixture was filtered through Celite and concentrated to afford 97, which was used in the next step without purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07645769B2
Source datasetuspto-grants-2010_01
ORD IDord-58326b8d41ae4f61a5d37376fe6aabfa
Source noteuspto-grants-2010_01