HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl (4-mercapto-2-methylphenoxy)acetate → 2,5-Dimethyl-4-mercaptophenoxy-acetic acid ethyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl (4-mercapto-2-methylphenoxy)acetate | HCID 16641178 | — |
| Reactant | Ethyl [4-(chlorosulfonyl)-2,5-dimethylphenoxy]acetate | HCID 20768123 | — |
| Product | 2,5-Dimethyl-4-mercaptophenoxy-acetic acid ethyl ester | HCID 20768107 | — |
Reaction Steps
The title compound was prepared according to the method described for preparing compound 10.3, using compound 21.2 as the starting material. 1H NMR (300 MHz) (CDCl3) δ 7.11 (1H, s); 6.54 (1H, s); 4.59 (2H, s); 4.26 (2H, q, J=7.2 Hz); 3.10 (1H, s); 2.29 (3H, s); 2.21 (3H, s); 1.30 (3H, t, J=7.2 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645779B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-57ed70ed97864bb5bc993d509dbdcdb7 |
| Source note | uspto-grants-2010_01 |