HCID 11312262, compound → HCID 11242358, compound

Participants

Reaction Steps

The compound was synthesized in 52% yield according to the procedure described for the synthesis of (7-dimethylsulfamoyl-benzimidazol-1-yl)-acetic acid, part C, starting from 2-{[2-nitro-6-(propylsulfonyl)phenyl]amino}ethanol. MS (ESI) m/z 259 [M+H]. 1H NMR (400 MHz, CDCl3/CD3OD) δ ppm 1.00 (t, J=7.3 Hz, 3H), 1.82-1.72 (m, 2H), 3.15-3.11 (m, 2H), 3.29-3.27 (m, 2H), 3.80-3.77 (m, 2H), 6.92-6.90 (m, 1H), 6.96 (t, J=7.8 Hz, 1H), 7.23 (dd, J=7.7, 1.6 Hz, 1H)

Provenance & Evidence