HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86608475, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 58728581 | HCID 58728581 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86608475 | HCID 86608475 | — |
Reaction Steps
Crude methyl 2,5-dichloro-3-{[(trifluoromethyl) sulfonyl]amino}benzoate (4.0 g) was dissolved in methanol (30 ml) and 4N NaOH (30 ml) was added while stirring at room temperature for 18 hrs. Removed solvent and added 4N HCl (10 ml). Stirred at room temperature for 4 hours. Filtered off solid to give 2,5-dichloro-3-{[(trifluoromethyl) sulfonyl]amino}benzoic acid hydrochloride in quantitative yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645771B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-1760d859c53c490999605a2e2098870e |
| Source note | uspto-grants-2010_01 |