HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178469423, compound → 6-fluoro-1H-1,2,3-benzotriazole-7-carboxylic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178469423 | HCID 178469423 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | 6-fluoro-1H-1,2,3-benzotriazole-7-carboxylic acid | HCID 178524663 | 90.1% |
Reaction Steps
ethyl 6-fluoro-1H-1,2,3-benzotriazole-7-carboxylate (920 mg) was heated in 6N HCl until all of the starting material disappeared. Evaporation of the HCl afforded 718 mg of a brownish solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645771B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-ff9efc54638b4c7f8f76bd61ed0e16db |
| Source note | uspto-grants-2010_01 |