HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Persulfate → HCID 58728611, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Persulfate | HCID 62655 | — |
| Reactant | 2-Amino-6-fluorobenzoic acid | HCID 521142 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 58728611 | HCID 58728611 | — |
Reaction Steps
2-amino-6-fluorobenzoic acid (5.00 g, 32.2 mmole) was dissolved in 30 ml of 2N sodium hydroxide. To this was added dropwise a solution of sodium persulfate (7.67 g, 32.2 mmole) in 80 ml of water. After stirring over night the resulting black solution was extracted with 2 L of ether and 1 L of ethylacetate. Evaporation of the water gave a black solid that was used with no purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07645771B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-77d702e545fc4dc2aead326567f18d31 |
| Source note | uspto-grants-2010_01 |