Hydrochloric Acid → HCID 131727847, compound

Participants

Reaction Steps

(2-{7-[3-(4-Cyanophenoxy)propyl]-9-oxa-3,7-diazabicyclo[3.3.1]non-3-yl}-ethyl)carbamic acid tert-butyl ester (4.5 g, 0.0104 mol; see step (i) above) was added to a solution of HCl in dioxane. The reaction was stirred at room temperature for 2 h, after which the reaction mixture was filtered and the resultant solid washed with dioxane, then diethyl ether and dried to give the title compound (3.89 g) as a white solid.

Provenance & Evidence