Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86761039 | HCID 86761039 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 86598852 | HCID 86598852 | — |
Reaction Steps
A solution of 18b (20 mg) in dry Et2O (1 mL) was treated at −8° C. with hydrochloric acid (1M in Et2O—0.5 mL). The resulting mixture was stirred at 0° C. for 10 minutes, then filtered; the filtrate was triturated with dry pentane (2×2 mL) to give the title compound as a whitish solid (14.7 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07648990B2 |
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| Source dataset | uspto-grants-2010_01 |
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| ORD ID | ord-3b000301dbb942a7a7af3536f00cad3a |
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| Source note | uspto-grants-2010_01 |
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