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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1992450Generated: October 30, 2026

Hydrochloric Acid → HCID 86598852, compound

https://huagongshe.com/reaction/1992450

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 86761039HCID 86761039—
SolventDiethyl EtherHCID 3283—
ProductHCID 86598852HCID 86598852—

Reaction Conditions

Temperature0 °C

Reaction Steps

A solution of 18b (20 mg) in dry Et2O (1 mL) was treated at −8° C. with hydrochloric acid (1M in Et2O—0.5 mL). The resulting mixture was stirred at 0° C. for 10 minutes, then filtered; the filtrate was triturated with dry pentane (2×2 mL) to give the title compound as a whitish solid (14.7 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07648990B2
Source datasetuspto-grants-2010_01
ORD IDord-3b000301dbb942a7a7af3536f00cad3a
Source noteuspto-grants-2010_01