HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 59716948, compound → HCID 68626046, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 59716948 | HCID 59716948 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 68626046 | HCID 68626046 | — |
Reaction Steps
A mixture of 1-benzyl-4-((1-methyl-4-phenylpiperidin-4-yl)methyl)piperazine (1.5 g, 4 mmol) and 20% PdOH/C in methanol (50 ml) was shaken in the hydrogenation bar under H2 50-60 psi for 18 hours. The mixture was then filtered and the solvent removed in vacuo to afford desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07649092B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-a87ff3b7f0374a728577690127ee05c4 |
| Source note | uspto-grants-2010_01 |