Hydrochloric Acid → HCID 68681026, compound

Participants

Reaction Steps

Experimental condition analogous to Example 13 were used with (2-Methyl-3-phenyl-allyl)-(2-piperidin-1-yl-ethyl)-amine, 0.5 g (1.9 mmol), 3,4,5-trimethoxy benzoic acid 0.49 g (2.3 mmol), 0.2 ml of triethylamine, O-(benzotriazol-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate 1.2 g (3.8 mmol). The reaction yielded 102 mg of an off-white solid as an HCl salt. Yield: 12%.

Provenance & Evidence