HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68714555, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 3,4,5-Trimethoxybenzoic Acid | HCID 8357 | — |
| Reactant | O-(Benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate | HCID 2733207 | — |
| Reactant | HCID 68700842 | HCID 68700842 | — |
| Product | HCID 68714555 | HCID 68714555 | 13% |
Reaction Steps
Experimental condition analogous to Example 13 were used with 3,4,5-trimethoxy benzoic acid, 0.65 g (3 mmol), and N,N-Dimethyl-N′-(2-methyl-3-phenyl-ally)-propane-1,3-diamine, 0.6 g (2.5 mmol) and O-(benzotriazole-1-yl)-N,N,N′,N′-tetramethyluronium tetrafluoroborate 1.5 g (5 mmol) to give 130 mg of a white solid as a HCl salt. Yield: 13%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07649011B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-da776fea018d40d19b046ead19ba4389 |
| Source note | uspto-grants-2010_01 |