Trifluoroacetic acid → HCID 72524890, compound

Participants

Reaction Steps

Experimental condition analogous to Example 12 were used with [2-bromo-3-(4-fluoro-phenyl)-allyl]-(1-cyclohexylmethyl-pyrrolidin-2-ylmethyl)-amine 0.15 g (0.36 mmol), 3,4,5-trimethoxy-benzoylchloride 0.1 g (0.47 mmol), and triethylamine 0.08 ml. Reverse phase high pressure liquid chromatography with a gradient of 20-80% acetonitrile phase lead to 120 mg of white powder as a TFA salt.

Provenance & Evidence