HCID 86616676, compound → HCID 68536290, compound

Participants

Reaction Steps

Synthesized in a manner similar to Example 46 (Step 7) using ethyl (2E)-3-{4-[(3-methyl-4-(methyloxy)-6-[(phenylmethyl)oxy]-2-{4-[(phenylmethyl)oxy]phenyl}-1-naphthalenyl)oxy]phenyl}-2-propenoate (257). 1H NMR (CDCl3, 300 MHz) δ 7.65 (d, J=9.1 Hz, 1H), 7.57 (d, J=16.0 Hz, 1H), 7.45-7.18 (m, 1H), 7.07 (dd, J=9.0, 2.5 Hz, 1H), 6.96 (d, J=8.5 Hz, 2H), 6.80 (d, J=8.7 Hz, 2H) 6.53 (d, J=8.6 Hz, 2H), 6.53 (d, J=8.6 Hz, 2H), 6.16 (d, J=16.0 Hz, 1H), 5.16 (s, 2H), 4.95 (s, 2H), 3.81 (s, 3H), 2.12 (s, 3H). LRMS (ESI) m/z 621 (M−1)−. TLC (90:10; CHCl3/MeOH): Rf=0.44.

Provenance & Evidence