HCID 86616677, compound → HCID 68534826, compound

Participants

Reaction Steps

Synthesized in a manner similar to Example 46 (Step 7) using ethyl (2E)-3-[4-({3-methyl-7-(methyloxy)-2-[4-(methyloxy)phenyl]-1-naphthalenyl}oxy)phenyl]-2-propenoate (265). 1H NMR (CDCl3, 400 MHz) δ 7.74 (d, J=9.0 Hz, 1H), 7.64 (d, J=15.9 Hz, 1H), 7.60 (s, 1H), 7.29 (d, J=8.8 Hz, 2H), 7.14 (dd, J=8.7, 2.4 Hz, 1H), 7.06-7.04 (m, 3H), 6.81 (d, J=8.7 Hz, 2H), 6.63 (d, J=8.7 Hz, 2H), 6.24 (d, J=15.9 Hz, 1H), 3.78 (s, 3H), 3.74 (s, 3H), 2.24 (s, 3H). TLC (90:10; CHCl3/MeOH): Rf=0.26.

Provenance & Evidence