HCID 68534826, compound → HCID 11632964, compound

Participants

Reaction Steps

Synthesized in a manner similar to Example 46 (Step 8) using (2E)-3-[4-({3-methyl-7-(methyloxy)-2-[4-(methyloxy)phenyl]-1-naphthalenyl}oxy)phenyl]-2-propenoic acid (266). 1H NMR (CD3OD, 400 MHz) δ 7.71 (d, J=8.6 Hz, 1H), 7.58 (s, 1H), 7.49 (d, J=15.5 Hz, 1H), 7.34 (d, J=8.4 Hz, 2H), 7.04 (dd, J=8.7, 2.0 Hz, 1H), 7.00 (s, 1H), 6.94 (d, J=8.5 Hz, 2H), 6.68 (d, J=8.4 Hz, 2H), 6.58 (d, J=8.4 Hz, 2H), 6.27 (d, J=15.2 Hz, 1H), 2.19 (s, 3H). TLC (90:10; CHCl3/MeOH): Rf=0.19.

Provenance & Evidence