HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Benzodioxole-4-carboxaldehyde → HCID 136102558, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Benzodioxole-4-carboxaldehyde | HCID 82264 | — |
| Reactant | 6-piperazin-1-yl-3H-pyrimidin-4-one | HCID 136102540 | — |
| Product | HCID 136102558 | HCID 136102558 | — |
Reaction Steps
6-(4-Benzo[1,3]dioxol-4-ylmethyl-piperazin-1-yl)-3H -pyrimidin-4-one was prepared using Procedure B from 6-piperazin-1-yl-3H-pyrimidin-4-one (Intermediate 4) and 2,3-(methylenedioxy)benzaldehyde (available from Aldrich). 1H NMR (400 MHz, CDCl3) δ 2.51-2.54 (m, 4H), 3.48-3.58 (m, 6H), 5.35 (s, 1H), 5.95 (s, 2H), 6.74-6.82 (m, 2H), 7.81 (s, 1H). Mass spectrum (ES) MH+=315.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652013B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-87d6f8e84355463f90284d2078eda117 |
| Source note | uspto-grants-2010_01 |