HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethyl)phenyl isocyanate → HCID 58659407, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethyl)phenyl isocyanate | HCID 9483 | — |
| Reactant | 4-{[2-(Trifluoromethyl)pyridin-4-yl]oxy}aniline | HCID 59134560 | — |
| Product | HCID 58659407 | HCID 58659407 | — |
Reaction Steps
The title compound is prepared as described in Example 102 but using 4-(2-trifluoromethyl-pyridin-4-yloxy)-phenylamine (Example 108) and α,α,α-trifluoro-m-tolyl-isocyanate. The reaction mixture is stirred for 4 h. The title compound is obtained as a white solid: ES-MS: 441.8 [M+H]+; single peak at tR=9.44 min (System 2); Rf=0.38 (CH2Cl2/Et2O, 90/10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652022B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-32b262638d7c4a86b7e8f9a6537830ba |
| Source note | uspto-grants-2010_01 |