HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Methylpiperazine → (4-Methyl-piperazin-1-yl)-(4-nitro-2-methoxy-phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Methylpiperazine | HCID 53167 | — |
| Reactant | 4-Nitro-o-anisic acid | HCID 75776 | — |
| Product | (4-Methyl-piperazin-1-yl)-(4-nitro-2-methoxy-phenyl)methanone | HCID 68541205 | — |
Reaction Steps
Prepared from 2-methoxy-4-nitrobenzoic acid and 1-methyl-piperazine (TPTU, CH2Cl2/CH3CN, Et3N): MS: [M+1]+=280; Anal.: CHN.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652022B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-9f4a9f2734264dd88bc2636e7ab80838 |
| Source note | uspto-grants-2010_01 |