HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 68535888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | 3-Nitro-5-(trifluoromethyl)benzoic acid | HCID 616602 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 68535888 | HCID 68535888 | — |
Reaction Steps
Prepared from 3-nitro-5-trifluormethyl-benzoic acid and piperidine (TPTU, CH2Cl2/CH3CN, Et3N): MS: [M+1]+=303; TLC Rf=0.27 (hexane/AcOEt 7:3).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652022B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-cd22f9bd15fb425da988ebe83480cc0b |
| Source note | uspto-grants-2010_01 |