HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23155228, compound → HCID 58659408, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23155228 | HCID 23155228 | — |
| Reactant | 4-Chloro-6-(4-isocyanatophenoxy)pyrimidine | HCID 57351767 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 58659408 | HCID 58659408 | — |
Reaction Steps
A solution of 4-chloro-6-(4-isocyanato-phenoxy)-pyrimidine (Stage 135.1; 594 mg; 2.40 mmol) in THF (2 ml) is mixed under a N2-atmosphere with a solution of 3-dimethylaminomethyl-5-trifluoromethyl-phenylamine (Stage 135.2; 524 mg; 2.40 mmol) in ether (10 ml). Stirring at rt affords the title compound: MS: [M+1]+=466.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07652022B2 |
| Source dataset | uspto-grants-2010_01 |
| ORD ID | ord-481dbb1ed6b146a1b7ddec2e404b250a |
| Source note | uspto-grants-2010_01 |