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HRID1993583

反应详情

EQUATION

反应方程式

HRID 1993583 的结构方程式

REACTANTS

反应物

1
结构：Cc1nccn1-c1ccc([N+](=O)[O-])cc1C(F)(F)F
HCID59822451

2-Methyl-1-[4-nitro-2-(trifluoromethyl)phenyl]-1H-imidazole

C11H8F3N3O2

PRODUCTS

生成物

1
结构：Cc1nccn1-c1ccc(N)cc1C(F)(F)F
HCID54935478

4-(2-Methyl-1H-imidazol-1-yl)-3-(trifluoromethyl)aniline

C11H10F3N3

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Ni]
催化剂HCID935

Nickel

Ni

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound is generated from 2-methyl-1-(4-nitro-2-trifluoromethyl-phenyl)-1H-imidazole (Stage 152.2) by hydrogenation in the presence of Raney-Ni in MeOH during 14 h at rt: Rf (MeOH/CH2Cl2=1:5): 0.42; M+H=242.0; m.p.=217-219° C.