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HRID1993584

反应详情

EQUATION

反应方程式

HRID 1993584 的结构方程式

REACTANTS

反应物

2
结构：Cc1ncc[nH]1
HCID12749

2-Methylimidazole

C4H6N2

结构：O=[N+]([O-])c1ccc(Br)c(C(F)(F)F)c1
HCID136198

2-Bromo-5-nitrobenzotrifluoride

C7H3BrF3NO2

PRODUCTS

生成物

1
结构：Cc1nccn1-c1ccc([N+](=O)[O-])cc1C(F)(F)F
HCID59822451

2-Methyl-1-[4-nitro-2-(trifluoromethyl)phenyl]-1H-imidazole

C11H8F3N3O2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CO.ClCCl
溶剂HCID21226129

未命名化合物

PROCEDURE

实验过程

The title compound is prepared by hearing 1-bromo-4-nitro-2-trifluoromethyl-benzene and 2-methyl-imidazole between 100-150° C. during 15 h: M+H=272.0; Rf (MeOH/CH2Cl2=1:5): 0.60.

WORKUP

后处理

  1. custombetween 100-150° C.
  2. customduring 15 h