Ammonium formate → HCID 68538057, compound

Participants

Reaction Conditions

Reaction Steps

Add ammonium formate (1.55 mmol, 0.1 g) and palladium (Carbon) 10% (0.031 mmol) over a solution of 2,2-dimethyl-1-[4-(4-methyl-5-nitro-pyridin-2-yl)-piperazin-1-yl]-propan-1-one (0.31 mmol, 0.09 g) in 2 mL of ethanol. Stir the solution for an hour at 90° C. Cool down and filter through a pad of Celite®, and concentrate under reduced pressure. Residue can be used without further purification. MS(ES): m/z=277 [M+H].

Provenance & Evidence